Exam Details
| Subject | pharmaceutical analysis – v | |
| Paper | ||
| Exam / Course | b. pharmacy | |
| Department | ||
| Organization | solapur university | |
| Position | ||
| Exam Date | 13, May, 2017 | |
| City, State | andhra pradesh, solapur |
Question Paper
B.Pharmacy (Semester VII) Examination, 2017
PHARMACEUTICAL ANALYSIS V
Day and Date Saturday, 13-5-2017 Total Marks 80
Time 3.00 p.m. to 6.00 p.m.
1. Multiple Choice Questions (16×1=16)
analysis where separation of sample mixture is done by
continuous addition of mobile phase.
Elution Displacement
Frontal None of these
Non-polar stationary phase is used in phase chromatography.
Reverse Normal
Isocratic All of these
is an example of paper used in paper chromatography.
Schull Edrol
Whatman All of the above
Mechanism of separation involved in TLC where silica gel G is used as
stationary phase and any organic solvent as mobile phase.
Adsorption Partition
Ion exchange reaction Molecular sieving
is used as a stationary phase in ion exchange
chromatography.
Zeolite Amberlite
Clay All of these
water is prepared by ion exchange chromatography.
Soft Deionised
Hard A and B
Which of the following is not used as stationary phase in gel
chromatography.
Agarose Sephadex
Bio-gel Amberlite
elution where varying composition of mobile phase is used.
Gradient Displacement
Isocratic A and B
Pore size of the stationary phase helps to separate sample mixtures in
chromatography.
Adsorption Gel
Ion exchange HPLC
10) is not a component of HPLC instrument.
Pump Solvent reservoir
Carrier gas Analytical column
11) detector is a solvent property detector used in HPLC.
Refractive index Infra red
Fluorescence UV-visible
12) ions are involved in ion exchange reaction in ion exchange
chromatography.
Fixed Counter
Mobile All of these
13) HETP is a Van deemter equation.
Au+B/u+Cu
A+B+Cu A+Bu+Cu
14) is an example of stationary phase used gas liquid
chromatography.
Polydimethyl siloxane Polyethylene glycol
A and B None of these
15) cannot be separated by gel chromatography.
Isomers Enantiomers
A and B None of these
16) Which of the following HPLC detector is highly temperature sensitive
I.R. Refractive index
ELSD None of these
2. Answer any four of the following questions.
Write on Height Equivalent to theoretical plate.
Write on ion exchange resins used in ion exchange chromatography.
Define the terms retention time and retention volume.
Draw a neat labeled diagram of gas chromatography. Give its advantages
and limitations.
Differentiate between TLC and HPTLC.
3. Answer any four of the following questions.
Give principle of ion exchange chromatography.
Write on different papers used in paper chromatography.
Write on different methods of column packing used in adsorption column
chromatography.
What is gel chromatography Give its principle.
Write a note on gas solid chromatography.
4. Answer any two of the following questions.
Write on columns and pumps used in HPLC.
Explain with suitable diagram any two detectors used in Gas Chromatography.
Explain various adsorbents used in adsorption column chromatography. Give
application of ion exchange chromatography.
5. Answer any two of the following questions.
Draw a neat labeled diagram of HPLC. Explain any two solute property detector
used in HPLC.
Write in detail on different development techniques used in paper and thin
layer chromatography.
Explain carrier gas and sample injection system used in Gas chromatography.
Give applications of it.
PHARMACEUTICAL ANALYSIS V
Day and Date Saturday, 13-5-2017 Total Marks 80
Time 3.00 p.m. to 6.00 p.m.
1. Multiple Choice Questions (16×1=16)
analysis where separation of sample mixture is done by
continuous addition of mobile phase.
Elution Displacement
Frontal None of these
Non-polar stationary phase is used in phase chromatography.
Reverse Normal
Isocratic All of these
is an example of paper used in paper chromatography.
Schull Edrol
Whatman All of the above
Mechanism of separation involved in TLC where silica gel G is used as
stationary phase and any organic solvent as mobile phase.
Adsorption Partition
Ion exchange reaction Molecular sieving
is used as a stationary phase in ion exchange
chromatography.
Zeolite Amberlite
Clay All of these
water is prepared by ion exchange chromatography.
Soft Deionised
Hard A and B
Which of the following is not used as stationary phase in gel
chromatography.
Agarose Sephadex
Bio-gel Amberlite
elution where varying composition of mobile phase is used.
Gradient Displacement
Isocratic A and B
Pore size of the stationary phase helps to separate sample mixtures in
chromatography.
Adsorption Gel
Ion exchange HPLC
10) is not a component of HPLC instrument.
Pump Solvent reservoir
Carrier gas Analytical column
11) detector is a solvent property detector used in HPLC.
Refractive index Infra red
Fluorescence UV-visible
12) ions are involved in ion exchange reaction in ion exchange
chromatography.
Fixed Counter
Mobile All of these
13) HETP is a Van deemter equation.
Au+B/u+Cu
A+B+Cu A+Bu+Cu
14) is an example of stationary phase used gas liquid
chromatography.
Polydimethyl siloxane Polyethylene glycol
A and B None of these
15) cannot be separated by gel chromatography.
Isomers Enantiomers
A and B None of these
16) Which of the following HPLC detector is highly temperature sensitive
I.R. Refractive index
ELSD None of these
2. Answer any four of the following questions.
Write on Height Equivalent to theoretical plate.
Write on ion exchange resins used in ion exchange chromatography.
Define the terms retention time and retention volume.
Draw a neat labeled diagram of gas chromatography. Give its advantages
and limitations.
Differentiate between TLC and HPTLC.
3. Answer any four of the following questions.
Give principle of ion exchange chromatography.
Write on different papers used in paper chromatography.
Write on different methods of column packing used in adsorption column
chromatography.
What is gel chromatography Give its principle.
Write a note on gas solid chromatography.
4. Answer any two of the following questions.
Write on columns and pumps used in HPLC.
Explain with suitable diagram any two detectors used in Gas Chromatography.
Explain various adsorbents used in adsorption column chromatography. Give
application of ion exchange chromatography.
5. Answer any two of the following questions.
Draw a neat labeled diagram of HPLC. Explain any two solute property detector
used in HPLC.
Write in detail on different development techniques used in paper and thin
layer chromatography.
Explain carrier gas and sample injection system used in Gas chromatography.
Give applications of it.
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- anatomy, physiology and health education – ii
- biochemistry
- biochemistry – i
- biochemistry – ii
- biopharmaceutics
- biotechnology
- clinical pharmacology
- herbal technology
- human anatomy and physiology – i
- human anatomy and physiology – ii
- medicinal chemistry – i
- medicinal chemistry – ii
- medicinal chemistry – iv
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- novel drug delivery systems
- organic chemistry – i
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- pathophysiology and clinical biochemistry – ii
- pharmaceutical analysis – i
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- pharmaceutical analysis – iv
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- pharmaceutical busines management
- pharmaceutical engineering
- pharmaceutical enginering
- pharmaceutical inorganic chemistry
- pharmaceutical jurisprudence
- pharmaceutical microbiology
- pharmaceutical organic chemistry – ii
- pharmaceutical organic chemistry –i
- pharmaceutics – i (new cbcs)
- pharmaceutics – i (old-cbcs pattern)
- pharmaceutics – ii
- pharmaceutics – iii
- pharmaceutics – iv
- pharmacognosy – i
- pharmacognosy – ii
- pharmacognosy – iii
- pharmacology – i (new) (cbcs pattern)
- pharmacology – ii
- pharmacology – ii (cgpa pattern)
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- physical pharmaceutics – i
- physical pharmacy – i
- physical pharmacy – ii
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