Exam Details
| Subject | pharmaceutical analysis – ii | |
| Paper | ||
| Exam / Course | b. pharmacy | |
| Department | ||
| Organization | solapur university | |
| Position | ||
| Exam Date | 15, May, 2017 | |
| City, State | andhra pradesh, solapur |
Question Paper
B.Pharmacy (Semester IV) (CGPA) Examination, 2017
PHARMACEUTICAL ANALYSIS II
Day and Date Monday, 15-5-2017 Total Marks 70
Time 3.00 p.m. to 6.00 p.m.
1. Multiple Choice Questions. (15×1=15)
is used as demasking agent.
Trimehanolamine Chloral hydrate
EDTA Hydroxylamine
introduces impurities in the precipitate.
Post precipitation Co-precipitation
Occlusion All of above
The sample prepared by mixing the increment is called
Sampling unit Increment
Gross sample Sub-sample
Ethylene diamine is type of solvent.
Aprotic Protophillic
Protogenic Amphiprotic
Composite sampling is used for sampling of
Solid Liquid
Gas None
End point detection in complexometric titrations is done by
Use of metal indicators Use of acid base indicators
Use of redox indicators All of above
is used as primary standard for standardization of perchloric
acid.
Potassium hydrogen pthalate Sodium hydroxide
Ascorbic acid Oxalic acid
The separation of element can be done by
Precipitation Volatilization
Electro-analytical method All of above
Digestion in the Kjeldahl's method is improved
Heating Addition of neutral salt
Addition of acid None
10) For estimation of iodine is used as absorbing liquid.
10 ml H2O 2 ml 1 N NaOH 1 ml H2O2 9 ml 1N H2SO4
20 ml H2O 20 ml 1 N NaOH
11) Eudiometer is used for the analysis of
Gas Solid
Liquid None
12) Potassium cyanide is used for the analysis of
All of above
13) ELIZA type of assay.
Fluorescence Enzyme
Both A and B None
14) For murexide pH is maintained.
2 3-4
6-7 10-11
15) The filter paper no are used for gelatinous and flocculent
precipitate.
40 and 540 42 and 542
41 and 541 40 and 30
2. Answer any five of the following questions.
Define digestion, precipition, Ostwald's ripening, sampling and gravimetry.
Explain in detail RIA.
Discuss in detail types of EDTA titrations.
Give the preparation and standardization of 0.1 N perchloric acid with its
principle behind it.
Write a note on gasometry.
Explain in detail discrete and composite sampling.
3. Answer any three of the following questions. (3×10=30)
Give an complete account of masking and demasking.
Explain in detail sampling of solid.
Enlist the steps involved in gravimetry and explain in detail precipitation
process.
Explain in detail oxygen flask combustion method.
PHARMACEUTICAL ANALYSIS II
Day and Date Monday, 15-5-2017 Total Marks 70
Time 3.00 p.m. to 6.00 p.m.
1. Multiple Choice Questions. (15×1=15)
is used as demasking agent.
Trimehanolamine Chloral hydrate
EDTA Hydroxylamine
introduces impurities in the precipitate.
Post precipitation Co-precipitation
Occlusion All of above
The sample prepared by mixing the increment is called
Sampling unit Increment
Gross sample Sub-sample
Ethylene diamine is type of solvent.
Aprotic Protophillic
Protogenic Amphiprotic
Composite sampling is used for sampling of
Solid Liquid
Gas None
End point detection in complexometric titrations is done by
Use of metal indicators Use of acid base indicators
Use of redox indicators All of above
is used as primary standard for standardization of perchloric
acid.
Potassium hydrogen pthalate Sodium hydroxide
Ascorbic acid Oxalic acid
The separation of element can be done by
Precipitation Volatilization
Electro-analytical method All of above
Digestion in the Kjeldahl's method is improved
Heating Addition of neutral salt
Addition of acid None
10) For estimation of iodine is used as absorbing liquid.
10 ml H2O 2 ml 1 N NaOH 1 ml H2O2 9 ml 1N H2SO4
20 ml H2O 20 ml 1 N NaOH
11) Eudiometer is used for the analysis of
Gas Solid
Liquid None
12) Potassium cyanide is used for the analysis of
All of above
13) ELIZA type of assay.
Fluorescence Enzyme
Both A and B None
14) For murexide pH is maintained.
2 3-4
6-7 10-11
15) The filter paper no are used for gelatinous and flocculent
precipitate.
40 and 540 42 and 542
41 and 541 40 and 30
2. Answer any five of the following questions.
Define digestion, precipition, Ostwald's ripening, sampling and gravimetry.
Explain in detail RIA.
Discuss in detail types of EDTA titrations.
Give the preparation and standardization of 0.1 N perchloric acid with its
principle behind it.
Write a note on gasometry.
Explain in detail discrete and composite sampling.
3. Answer any three of the following questions. (3×10=30)
Give an complete account of masking and demasking.
Explain in detail sampling of solid.
Enlist the steps involved in gravimetry and explain in detail precipitation
process.
Explain in detail oxygen flask combustion method.
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Subjects
- anatomy, physiology and health education – i
- anatomy, physiology and health education – ii
- biochemistry
- biochemistry – i
- biochemistry – ii
- biopharmaceutics
- biotechnology
- clinical pharmacology
- herbal technology
- human anatomy and physiology – i
- human anatomy and physiology – ii
- medicinal chemistry – i
- medicinal chemistry – ii
- medicinal chemistry – iv
- microbiology
- modern dispensing and hospital pharmacy
- novel drug delivery systems
- organic chemistry – i
- organic chemistry – ii
- organic chemistry – iii
- pathophysiology (new cbcs)
- pathophysiology and clinical biochemistry – i
- pathophysiology and clinical biochemistry – ii
- pharmaceutical analysis – i
- pharmaceutical analysis – ii
- pharmaceutical analysis – iv
- pharmaceutical analysis – v
- pharmaceutical analysis – vi
- pharmaceutical busines management
- pharmaceutical engineering
- pharmaceutical enginering
- pharmaceutical inorganic chemistry
- pharmaceutical jurisprudence
- pharmaceutical microbiology
- pharmaceutical organic chemistry – ii
- pharmaceutical organic chemistry –i
- pharmaceutics – i (new cbcs)
- pharmaceutics – i (old-cbcs pattern)
- pharmaceutics – ii
- pharmaceutics – iii
- pharmaceutics – iv
- pharmacognosy – i
- pharmacognosy – ii
- pharmacognosy – iii
- pharmacology – i (new) (cbcs pattern)
- pharmacology – ii
- pharmacology – ii (cgpa pattern)
- pharmacology – iv
- physical pharmaceutics – i
- physical pharmacy – i
- physical pharmacy – ii
- sterile dosage forms