Exam Details
| Subject | pharmaceutical analysis – ii | |
| Paper | ||
| Exam / Course | b. pharmacy | |
| Department | ||
| Organization | solapur university | |
| Position | ||
| Exam Date | November, 2017 | |
| City, State | andhra pradesh, solapur |
Question Paper
B.Pharm. (Semester IV) (CGPA) Examination, 2017
PHARMACEUTICAL ANALYSIS II
Day and Date Thursday, 7-12-2017 Max. Marks 70
Time 3.00 p.m. to 6.00 p.m.
1. Multiple Choice Questions (1×15=15)
Aromatic amine and nitrous acid reaction gives formation of
Diazonium salt Sodium nitrite
Phenol No reaction
is used as titrant in non aqueous titration.
Perchloric acid EDTA
Sodium nitrite Silver nitrite
Principle of gravimetric analysis based on
Precipitation Volatization
Electro analytical All of the above
Assay of sulphanilamide is Titration.
Diazotization Sodium nitrite
Both and None of the above
external indicator in sodium nitrite titration.
Starch iodide paper Starch powder
Iodine solution Starch solution
By oxygen flask combustion technique determination of is done.
Nitrogen Halogen
Moisture Acid
Substance which releases masked metal ion is called
Masking agent Demasking agent
Complexing agent Chelating agent
K.F.R. reagent consists
I2 SO2 Pyridine I2 SO2 Pyridine Methanol
I2 SO2 Methanol I2 SO2
The platinum wire fused in Oxygen flask stopper is
13 12 11 14
10) Kjeldahl method is used for the estimation of
Nitrogen Oxygen Hydrogen Halogen
11) Ascorbic acid is used as masking agent for
Mg Mn Ni Cu
12) Assay of Norfloxacin is type of titration.
Aqueous Non Aqueous
Precipitation Complexometric
13) Non aqueous solvent having property.
Self dissociation Dielectric constant
Acid base characteristics All of the above
14) ELISA is a type of
Enzyme Fluorescence
Both None
15) Benzene is solvent.
Protogenic Protophilic
Aprotic Amphiprotic
2. Answer any five
Explain the principle and applications of radioimmunoassay.
Write about masking and demasking agent with example.
Give complete account of non aqueous solvents.
Write note on sampling of solids.
Define gravimetry. Explain assay of zinc sulphate by gravimetry.
With the mechanism explain three Metallochrome indicators.
3. Answer any three of following (10×3=30)
Explain in detail Kjeldahl method and gasometry.
Explain in detail Karl Fischer method.
Describe the steps involved in gravimetric analysis.
Give the preparation and standardization of 0.1 M NaNO2. Explain in detail
end point detection in nitrite titration.
PHARMACEUTICAL ANALYSIS II
Day and Date Thursday, 7-12-2017 Max. Marks 70
Time 3.00 p.m. to 6.00 p.m.
1. Multiple Choice Questions (1×15=15)
Aromatic amine and nitrous acid reaction gives formation of
Diazonium salt Sodium nitrite
Phenol No reaction
is used as titrant in non aqueous titration.
Perchloric acid EDTA
Sodium nitrite Silver nitrite
Principle of gravimetric analysis based on
Precipitation Volatization
Electro analytical All of the above
Assay of sulphanilamide is Titration.
Diazotization Sodium nitrite
Both and None of the above
external indicator in sodium nitrite titration.
Starch iodide paper Starch powder
Iodine solution Starch solution
By oxygen flask combustion technique determination of is done.
Nitrogen Halogen
Moisture Acid
Substance which releases masked metal ion is called
Masking agent Demasking agent
Complexing agent Chelating agent
K.F.R. reagent consists
I2 SO2 Pyridine I2 SO2 Pyridine Methanol
I2 SO2 Methanol I2 SO2
The platinum wire fused in Oxygen flask stopper is
13 12 11 14
10) Kjeldahl method is used for the estimation of
Nitrogen Oxygen Hydrogen Halogen
11) Ascorbic acid is used as masking agent for
Mg Mn Ni Cu
12) Assay of Norfloxacin is type of titration.
Aqueous Non Aqueous
Precipitation Complexometric
13) Non aqueous solvent having property.
Self dissociation Dielectric constant
Acid base characteristics All of the above
14) ELISA is a type of
Enzyme Fluorescence
Both None
15) Benzene is solvent.
Protogenic Protophilic
Aprotic Amphiprotic
2. Answer any five
Explain the principle and applications of radioimmunoassay.
Write about masking and demasking agent with example.
Give complete account of non aqueous solvents.
Write note on sampling of solids.
Define gravimetry. Explain assay of zinc sulphate by gravimetry.
With the mechanism explain three Metallochrome indicators.
3. Answer any three of following (10×3=30)
Explain in detail Kjeldahl method and gasometry.
Explain in detail Karl Fischer method.
Describe the steps involved in gravimetric analysis.
Give the preparation and standardization of 0.1 M NaNO2. Explain in detail
end point detection in nitrite titration.
Other Question Papers
Subjects
- anatomy, physiology and health education – i
- anatomy, physiology and health education – ii
- biochemistry
- biochemistry – i
- biochemistry – ii
- biopharmaceutics
- biotechnology
- clinical pharmacology
- herbal technology
- human anatomy and physiology – i
- human anatomy and physiology – ii
- medicinal chemistry – i
- medicinal chemistry – ii
- medicinal chemistry – iv
- microbiology
- modern dispensing and hospital pharmacy
- novel drug delivery systems
- organic chemistry – i
- organic chemistry – ii
- organic chemistry – iii
- pathophysiology (new cbcs)
- pathophysiology and clinical biochemistry – i
- pathophysiology and clinical biochemistry – ii
- pharmaceutical analysis – i
- pharmaceutical analysis – ii
- pharmaceutical analysis – iv
- pharmaceutical analysis – v
- pharmaceutical analysis – vi
- pharmaceutical busines management
- pharmaceutical engineering
- pharmaceutical enginering
- pharmaceutical inorganic chemistry
- pharmaceutical jurisprudence
- pharmaceutical microbiology
- pharmaceutical organic chemistry – ii
- pharmaceutical organic chemistry –i
- pharmaceutics – i (new cbcs)
- pharmaceutics – i (old-cbcs pattern)
- pharmaceutics – ii
- pharmaceutics – iii
- pharmaceutics – iv
- pharmacognosy – i
- pharmacognosy – ii
- pharmacognosy – iii
- pharmacology – i (new) (cbcs pattern)
- pharmacology – ii
- pharmacology – ii (cgpa pattern)
- pharmacology – iv
- physical pharmaceutics – i
- physical pharmacy – i
- physical pharmacy – ii
- sterile dosage forms