Exam Details
| Subject | pharmaceutical analysis – ii | |
| Paper | ||
| Exam / Course | b. pharmacy | |
| Department | ||
| Organization | solapur university | |
| Position | ||
| Exam Date | March, 2018 | |
| City, State | andhra pradesh, solapur |
Question Paper
B. Pharmacy (Semester Examination, 2018
(CGPA)
PHARMACEUTICAL ANALYSIS III
Day and Date Saturday, 12-5-2018 Total Marks 70
Time 10.30 a.m. to 1.30 p.m.
1. Multiple choice questions (15×1=15)
In spectrofluorimeter light source is
Mercury vapour lamp Xenon arc lamp
Both and H2 lamp
Re-emission of previously absorbed radiation is phenomenon of
Scattering
Atomic absorption spectrophotometer
Luminescence
Absorbance
The commonly used detector in the UV spectrophotometer is
Photomultiplier tube Thermocouple
Bolometer Littro Prisms
is used for dispersing the incident radiation in UV spectroscopy.
Nicol Prism Diffraction grating
Both and None
UV-Visible spectroscopy is a type of
Atomic absorption spectroscopy
Atomic emission spectroscopy
Molecular spectroscopy
Magnetic spectroscopy
Electromagnetic radiation in the wavelength range 2.5 to 15 micron is
UV spectrum I.R.
X ray Visible
solvent does not absorb UV radiation.
Water Heptene
Ethylene All of above
Reciprocal wavelength is
Speed Wave number
Frequency Velocity
1A°
10-4 cm 10-1 cm
10-4 centipoises 10-8 cm
10) The U.V. radiation has more energy than
Microwave Gamma ray
Both and None
11) Absorbtion of energy by ground state atoms in gaseous state forms the basis of
AES FES
AFE AAS
12) Sample to be analyzed by atomic absorption must be vaporized or atomized by using
Flame atomiser Non flame atomizers
and None
13) is used as detector in AAS.
PVC PMT
Silicon crystal Ruby crystal
14) interferences occurs in AAS.
Spectral Chemical
None and
15) °C temp. is achieved from acetylene and air.
2600 2200
45000 2800
2. Answer any five
Illustrate EMS.
Enlist various methods of assay of substances in multi component samples. Derive simultaneous equation method.
What do you mean by fluorescence and phosphorescence Draw a neat labeled diagram of filter fluorimeter.
Write a note on instrumental parameter required for spectroscopic measurements.
Enlist various atomizer used in AAS. Discuss in detail total consumption burner.
Give applications of flame photometry.
3. Answer any three (3×10=30)
Draw neat labelled diagram of a double beam UV Spectrophotometer. Explain the detector and sources used in UV Spectrophotometer.
Discuss principle, instrumentation and working of AAS with a neat labelled diagram.
Explain in detail energy level diagram. Give advantages of fluorescence spectroscopy.
Give in detail factors affecting fluorescence intensity.
(CGPA)
PHARMACEUTICAL ANALYSIS III
Day and Date Saturday, 12-5-2018 Total Marks 70
Time 10.30 a.m. to 1.30 p.m.
1. Multiple choice questions (15×1=15)
In spectrofluorimeter light source is
Mercury vapour lamp Xenon arc lamp
Both and H2 lamp
Re-emission of previously absorbed radiation is phenomenon of
Scattering
Atomic absorption spectrophotometer
Luminescence
Absorbance
The commonly used detector in the UV spectrophotometer is
Photomultiplier tube Thermocouple
Bolometer Littro Prisms
is used for dispersing the incident radiation in UV spectroscopy.
Nicol Prism Diffraction grating
Both and None
UV-Visible spectroscopy is a type of
Atomic absorption spectroscopy
Atomic emission spectroscopy
Molecular spectroscopy
Magnetic spectroscopy
Electromagnetic radiation in the wavelength range 2.5 to 15 micron is
UV spectrum I.R.
X ray Visible
solvent does not absorb UV radiation.
Water Heptene
Ethylene All of above
Reciprocal wavelength is
Speed Wave number
Frequency Velocity
1A°
10-4 cm 10-1 cm
10-4 centipoises 10-8 cm
10) The U.V. radiation has more energy than
Microwave Gamma ray
Both and None
11) Absorbtion of energy by ground state atoms in gaseous state forms the basis of
AES FES
AFE AAS
12) Sample to be analyzed by atomic absorption must be vaporized or atomized by using
Flame atomiser Non flame atomizers
and None
13) is used as detector in AAS.
PVC PMT
Silicon crystal Ruby crystal
14) interferences occurs in AAS.
Spectral Chemical
None and
15) °C temp. is achieved from acetylene and air.
2600 2200
45000 2800
2. Answer any five
Illustrate EMS.
Enlist various methods of assay of substances in multi component samples. Derive simultaneous equation method.
What do you mean by fluorescence and phosphorescence Draw a neat labeled diagram of filter fluorimeter.
Write a note on instrumental parameter required for spectroscopic measurements.
Enlist various atomizer used in AAS. Discuss in detail total consumption burner.
Give applications of flame photometry.
3. Answer any three (3×10=30)
Draw neat labelled diagram of a double beam UV Spectrophotometer. Explain the detector and sources used in UV Spectrophotometer.
Discuss principle, instrumentation and working of AAS with a neat labelled diagram.
Explain in detail energy level diagram. Give advantages of fluorescence spectroscopy.
Give in detail factors affecting fluorescence intensity.
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Subjects
- anatomy, physiology and health education – i
- anatomy, physiology and health education – ii
- biochemistry
- biochemistry – i
- biochemistry – ii
- biopharmaceutics
- biotechnology
- clinical pharmacology
- herbal technology
- human anatomy and physiology – i
- human anatomy and physiology – ii
- medicinal chemistry – i
- medicinal chemistry – ii
- medicinal chemistry – iv
- microbiology
- modern dispensing and hospital pharmacy
- novel drug delivery systems
- organic chemistry – i
- organic chemistry – ii
- organic chemistry – iii
- pathophysiology (new cbcs)
- pathophysiology and clinical biochemistry – i
- pathophysiology and clinical biochemistry – ii
- pharmaceutical analysis – i
- pharmaceutical analysis – ii
- pharmaceutical analysis – iv
- pharmaceutical analysis – v
- pharmaceutical analysis – vi
- pharmaceutical busines management
- pharmaceutical engineering
- pharmaceutical enginering
- pharmaceutical inorganic chemistry
- pharmaceutical jurisprudence
- pharmaceutical microbiology
- pharmaceutical organic chemistry – ii
- pharmaceutical organic chemistry –i
- pharmaceutics – i (new cbcs)
- pharmaceutics – i (old-cbcs pattern)
- pharmaceutics – ii
- pharmaceutics – iii
- pharmaceutics – iv
- pharmacognosy – i
- pharmacognosy – ii
- pharmacognosy – iii
- pharmacology – i (new) (cbcs pattern)
- pharmacology – ii
- pharmacology – ii (cgpa pattern)
- pharmacology – iv
- physical pharmaceutics – i
- physical pharmacy – i
- physical pharmacy – ii
- sterile dosage forms