Exam Details
| Subject | pharmaceutical analysis – ii | |
| Paper | ||
| Exam / Course | b. pharmacy | |
| Department | ||
| Organization | solapur university | |
| Position | ||
| Exam Date | March, 2018 | |
| City, State | andhra pradesh, solapur |
Question Paper
B.Pharm. (Semester IV) (New CBCS) Examination, 2018
Pharmaceutical Analysis II
Day and Date Monday, 14-5-2018 Max. Marks 70
Time 3.00 p.m. to 6.00 p.m.
1. Choose the correct alternative (1×15=15)
The pH is maintained in direct EDTA titration.
1 5 15 10
In Perchloric acid standardization is used as primary standard.
NaOH Na2CO3
PHT None of the above
Mureoxide is used for determination of
The particle size of precipitate is controlled by
Solubility of precipitate in medium
Concentration of reactant
Temperature
All of the above
For chlorine absorbing liquid is
Sodium hydroxide Sulphuric acid
Bromine Silver nitrate
Eudiometer is used for analysis of
Gas Solid
Liquid None of the above
Protophilic solvents are nature.
Acidic Basic
Neutral Both and
indicator is generally used for non-aqueous titration.
Crystal violet Mordant black II
Catechol violet Starch
For fluorine is absorbing liquid used.
Water Sodium hydroxide
Hydrogen peroxide None of the above
P.T.O.
Seat
No.
Set
P
Set P
SLR-TA 28 *SLRTA28*
10) Karl Fischer reagent is used for determination of
Halogen Nitrogen
Water None of the above
11) At pH 10 mordant black shows color.
Pink Blue Red Yellow
12) Filter paper no. 42 is generally used for particles.
Fine Very fine
Coarse particles None of the above
13) Above 500°C types of tubes are preferable for sampling of gases.
Hard glass tube Silica quartz tube
Glass tube None of the above
14) 18.6 gm of Disodium EDTA in 1000 ml distilled water is M.
0.1 1 2 0.5
15) gm sodium nitrite in 1000 ml distilled water is 0.1 M.
8.6 gm 8.00 gm 6.8 gm 6.00 gm
2. Answer any five
Explain end point detection in complexometric titrations. Write a note on Metallochrome indicators.
Define non-aqueous titration. Give the preparation and standardization of 0.1 N Perchloric acids.
Write a note on Radio-immune assay.
Explain assay of Mebendazole and enlist types of non-aqueous solvents.
What is Co-precipitation Explain different types of Co-precipitation.
Define Masking and Demasking agents. Explain assay of calcium gluconate inj.
3. Answer any three of followings (10×3=30)
Define complexometric titration. Give the preparation and standardization of 0.05 M disodium EDTA and explain assay of Magnesium sulphate.
Define raw material and give types of raw materials. Explain raw material analysis of starch.
Explain the assay Norfloxacin powder and calcium gluconate powder with factor calculation.
Explain in brief ELISA method.
Pharmaceutical Analysis II
Day and Date Monday, 14-5-2018 Max. Marks 70
Time 3.00 p.m. to 6.00 p.m.
1. Choose the correct alternative (1×15=15)
The pH is maintained in direct EDTA titration.
1 5 15 10
In Perchloric acid standardization is used as primary standard.
NaOH Na2CO3
PHT None of the above
Mureoxide is used for determination of
The particle size of precipitate is controlled by
Solubility of precipitate in medium
Concentration of reactant
Temperature
All of the above
For chlorine absorbing liquid is
Sodium hydroxide Sulphuric acid
Bromine Silver nitrate
Eudiometer is used for analysis of
Gas Solid
Liquid None of the above
Protophilic solvents are nature.
Acidic Basic
Neutral Both and
indicator is generally used for non-aqueous titration.
Crystal violet Mordant black II
Catechol violet Starch
For fluorine is absorbing liquid used.
Water Sodium hydroxide
Hydrogen peroxide None of the above
P.T.O.
Seat
No.
Set
P
Set P
SLR-TA 28 *SLRTA28*
10) Karl Fischer reagent is used for determination of
Halogen Nitrogen
Water None of the above
11) At pH 10 mordant black shows color.
Pink Blue Red Yellow
12) Filter paper no. 42 is generally used for particles.
Fine Very fine
Coarse particles None of the above
13) Above 500°C types of tubes are preferable for sampling of gases.
Hard glass tube Silica quartz tube
Glass tube None of the above
14) 18.6 gm of Disodium EDTA in 1000 ml distilled water is M.
0.1 1 2 0.5
15) gm sodium nitrite in 1000 ml distilled water is 0.1 M.
8.6 gm 8.00 gm 6.8 gm 6.00 gm
2. Answer any five
Explain end point detection in complexometric titrations. Write a note on Metallochrome indicators.
Define non-aqueous titration. Give the preparation and standardization of 0.1 N Perchloric acids.
Write a note on Radio-immune assay.
Explain assay of Mebendazole and enlist types of non-aqueous solvents.
What is Co-precipitation Explain different types of Co-precipitation.
Define Masking and Demasking agents. Explain assay of calcium gluconate inj.
3. Answer any three of followings (10×3=30)
Define complexometric titration. Give the preparation and standardization of 0.05 M disodium EDTA and explain assay of Magnesium sulphate.
Define raw material and give types of raw materials. Explain raw material analysis of starch.
Explain the assay Norfloxacin powder and calcium gluconate powder with factor calculation.
Explain in brief ELISA method.
Other Question Papers
Subjects
- anatomy, physiology and health education – i
- anatomy, physiology and health education – ii
- biochemistry
- biochemistry – i
- biochemistry – ii
- biopharmaceutics
- biotechnology
- clinical pharmacology
- herbal technology
- human anatomy and physiology – i
- human anatomy and physiology – ii
- medicinal chemistry – i
- medicinal chemistry – ii
- medicinal chemistry – iv
- microbiology
- modern dispensing and hospital pharmacy
- novel drug delivery systems
- organic chemistry – i
- organic chemistry – ii
- organic chemistry – iii
- pathophysiology (new cbcs)
- pathophysiology and clinical biochemistry – i
- pathophysiology and clinical biochemistry – ii
- pharmaceutical analysis – i
- pharmaceutical analysis – ii
- pharmaceutical analysis – iv
- pharmaceutical analysis – v
- pharmaceutical analysis – vi
- pharmaceutical busines management
- pharmaceutical engineering
- pharmaceutical enginering
- pharmaceutical inorganic chemistry
- pharmaceutical jurisprudence
- pharmaceutical microbiology
- pharmaceutical organic chemistry – ii
- pharmaceutical organic chemistry –i
- pharmaceutics – i (new cbcs)
- pharmaceutics – i (old-cbcs pattern)
- pharmaceutics – ii
- pharmaceutics – iii
- pharmaceutics – iv
- pharmacognosy – i
- pharmacognosy – ii
- pharmacognosy – iii
- pharmacology – i (new) (cbcs pattern)
- pharmacology – ii
- pharmacology – ii (cgpa pattern)
- pharmacology – iv
- physical pharmaceutics – i
- physical pharmacy – i
- physical pharmacy – ii
- sterile dosage forms