Exam Details
| Subject | pharmaceutical analysis – i | |
| Paper | ||
| Exam / Course | b. pharmacy | |
| Department | ||
| Organization | solapur university | |
| Position | ||
| Exam Date | October, 2018 | |
| City, State | andhra pradesh, solapur |
Question Paper
B.Pharmacy (Semester III) (Old CBCS Pattern) Examination, 2018
pharmaceutical analysis i
Day and Date Thursday, 27-12-2018 Total Marks 70
Time 2.30 p.m. to 5.30 p.m.
1. MCQ 15
Standardization of Iodine is carried out using
Sodium thiosulphate
Oxalic acid
Perchloric acid
None of these
IM H2SO4 N H2SO4.
1 2
0.5 0.1
The tolerance capacity for one mark 10 ml pipette as per I.P. is ml.
0.02 0.005
0.01 0.001
In Redox titration is used as primary standard.
Sodium carbonate
Potassium bromate
Potassium hydrogen phthalate
All
The degree of agreement between measured value and accepted true
value is
Precision Accuracy
Range Average deviation
Acidic Dye used in Fajan's series is
Eosin Rhodamine series
Floroscein Both and
P.T.O.
P
Set P
Gasometric analysis determines gases.
Cyclopropane Amyl Nitrate
Octyl Nitrate All
Phenolphthalein has pH range of
6.8 to 8.4 1.2 to 2.8
8.3 to 11.0 4.2 to 6.3
Drug which is not titrated by Volhard's method is
Aminophylline Potassium chloride
Thiomersal Sulphobromophthalein sodium
10) Behavior of indicator is explained by theory.
Chromospheres Ionic
Color Resonance
11) pH is defined as
-log -log
pH pOH log pOH
12) The titration carries out between KCl and AgNO3 is termed as
titration.
Oxidation-Reduction Precipitation
Acid-Base None of these
13) Approx. quantity of Indicators used in titration is of solution
being titrated.
0.0001 to 0.0004 0.0004 to 0.0008
0.01 to 0.02% 0.001 to 0.004
14) Molecular weight of isoniazide power as per I.P. is gm.
136.02 138.10 138.90 137.14
15) 8.5 ml HCl in 1 litre
0.1 M 0.1 N
Both and 0.5 M
2. Answer any 5 25
Write a note on preparation and standardization of 0.05 M cerric ammonium
sulphate.
Write a note on redox titrations.
SLR-TV 22 *SLRTV22*
Set P
Define accuracy, presision, significant figures, relative errors, mole
fraction.
Explain Neutralization curve for strong acid and strong base.
Explain solubility product and common ion effect.
Explain in detail turbidity method.
3. Answer any 3 30
Explain Fajan's method. Add a note on behavior of indicators.
Explain law of mass action. Write a note on principle involved in NaCl
injection I.P.
Explain Volhard's method. How will you overcome the problems during
Volhard's method
Explain errors with suitable examples. How will you determine the
percentage purity of aspirin powder I.P.
pharmaceutical analysis i
Day and Date Thursday, 27-12-2018 Total Marks 70
Time 2.30 p.m. to 5.30 p.m.
1. MCQ 15
Standardization of Iodine is carried out using
Sodium thiosulphate
Oxalic acid
Perchloric acid
None of these
IM H2SO4 N H2SO4.
1 2
0.5 0.1
The tolerance capacity for one mark 10 ml pipette as per I.P. is ml.
0.02 0.005
0.01 0.001
In Redox titration is used as primary standard.
Sodium carbonate
Potassium bromate
Potassium hydrogen phthalate
All
The degree of agreement between measured value and accepted true
value is
Precision Accuracy
Range Average deviation
Acidic Dye used in Fajan's series is
Eosin Rhodamine series
Floroscein Both and
P.T.O.
P
Set P
Gasometric analysis determines gases.
Cyclopropane Amyl Nitrate
Octyl Nitrate All
Phenolphthalein has pH range of
6.8 to 8.4 1.2 to 2.8
8.3 to 11.0 4.2 to 6.3
Drug which is not titrated by Volhard's method is
Aminophylline Potassium chloride
Thiomersal Sulphobromophthalein sodium
10) Behavior of indicator is explained by theory.
Chromospheres Ionic
Color Resonance
11) pH is defined as
-log -log
pH pOH log pOH
12) The titration carries out between KCl and AgNO3 is termed as
titration.
Oxidation-Reduction Precipitation
Acid-Base None of these
13) Approx. quantity of Indicators used in titration is of solution
being titrated.
0.0001 to 0.0004 0.0004 to 0.0008
0.01 to 0.02% 0.001 to 0.004
14) Molecular weight of isoniazide power as per I.P. is gm.
136.02 138.10 138.90 137.14
15) 8.5 ml HCl in 1 litre
0.1 M 0.1 N
Both and 0.5 M
2. Answer any 5 25
Write a note on preparation and standardization of 0.05 M cerric ammonium
sulphate.
Write a note on redox titrations.
SLR-TV 22 *SLRTV22*
Set P
Define accuracy, presision, significant figures, relative errors, mole
fraction.
Explain Neutralization curve for strong acid and strong base.
Explain solubility product and common ion effect.
Explain in detail turbidity method.
3. Answer any 3 30
Explain Fajan's method. Add a note on behavior of indicators.
Explain law of mass action. Write a note on principle involved in NaCl
injection I.P.
Explain Volhard's method. How will you overcome the problems during
Volhard's method
Explain errors with suitable examples. How will you determine the
percentage purity of aspirin powder I.P.
Other Question Papers
Subjects
- anatomy, physiology and health education – i
- anatomy, physiology and health education – ii
- biochemistry
- biochemistry – i
- biochemistry – ii
- biopharmaceutics
- biotechnology
- clinical pharmacology
- herbal technology
- human anatomy and physiology – i
- human anatomy and physiology – ii
- medicinal chemistry – i
- medicinal chemistry – ii
- medicinal chemistry – iv
- microbiology
- modern dispensing and hospital pharmacy
- novel drug delivery systems
- organic chemistry – i
- organic chemistry – ii
- organic chemistry – iii
- pathophysiology (new cbcs)
- pathophysiology and clinical biochemistry – i
- pathophysiology and clinical biochemistry – ii
- pharmaceutical analysis – i
- pharmaceutical analysis – ii
- pharmaceutical analysis – iv
- pharmaceutical analysis – v
- pharmaceutical analysis – vi
- pharmaceutical busines management
- pharmaceutical engineering
- pharmaceutical enginering
- pharmaceutical inorganic chemistry
- pharmaceutical jurisprudence
- pharmaceutical microbiology
- pharmaceutical organic chemistry – ii
- pharmaceutical organic chemistry –i
- pharmaceutics – i (new cbcs)
- pharmaceutics – i (old-cbcs pattern)
- pharmaceutics – ii
- pharmaceutics – iii
- pharmaceutics – iv
- pharmacognosy – i
- pharmacognosy – ii
- pharmacognosy – iii
- pharmacology – i (new) (cbcs pattern)
- pharmacology – ii
- pharmacology – ii (cgpa pattern)
- pharmacology – iv
- physical pharmaceutics – i
- physical pharmacy – i
- physical pharmacy – ii
- sterile dosage forms